LiNi 0.5 Mn 1.5 O 4 powder was successfully synthesised via ball-milling, followed by calcination at temperatures of 750, 850 and 950 °C. The physical and electrochemical properties of LiNi 0.5 Mn 1.5 O 4 powder were characterised by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and galvanostatic charge/discharge. At a 1 C rate, LiNi 0.5 Mn 1.5 …